The results show that when the molar ratio of methyl indole-6-carboxylate to DMF and NaOH is 1∶8∶4,the yields of 1 is 54.
4-甲基-3-硝基苯甲酸经MeOH/H2SO4酯化得4-甲基-3-硝基苯甲酸甲酯(2),2与N,N-二甲基甲酰胺二甲基缩醛缩合后经Fe/HAc还原制得吲哚-6-甲酸甲酯(3),最后3与POCl3/DMF通过Vilsmeier反应合成了3-醛基吲哚-6-甲酸(1)。
Synthesis and Biological Activities of N-(3-Substituted Benzenesulfonamido) Benzenesulfonyl-6-Methylindole Derivatives
N-（3-取代苯磺酰氨基）苯磺酰基-6-甲基吲哚类化合物合成及生物活性研究
Synthesis of 1,3,3,5-tetramethyl-6-nitro-indoline spiroben-zopyrans
1,3,3,5-四甲基-6-硝基吲哚啉螺苯并吡喃的合成
THE ACTION OF HYDROGEN PEROXIDE TOWARDS 2-METHYL-3- (β-DIETHYLAMINOETHYL) INDOLE
?氧化???-甲基-3-(β-二乙胺乙基)吲哚的作用
Synthesis of N-(methyl-phenyl) benzo Indole
N-(对甲基苯基)苯并吲哚的合成研究
Synthesis of Dye Intermediate 2,3,3-Trimethyl-3H-Indole;
染料中间体2,3,3-三甲基-3H-吲哚的合成
diindolyl-4-phridyl methane
二吲哚-4-吡啶甲烷
Rose Bengal Sensitized Singlet Oxygenation of 1 - Methyl - 2 - phenylindole
1-甲基-2-苯基吲哚的琥红敏化单重态氧反应
Synthesis of 1-Hydroxy-1-methyl-3-oxo-isoindole Derivatives
1-羟基-1-甲基-3-氧-异吲哚类衍生物的合成
Synthesis and Characterization of 3-(1-chloro-2,2-dimethylpropylidene) indolin-2-one
3-(1-氯-2,2-二甲基)亚丙基)吲哚酮的合成与表征
Mass Analyzed Threshold Ionization Spectroscopy of Bromopropanes and Methylindoles;
溴丙烷及甲基吲哚的质量分辨零动能光谱研究
New Derivatives I3C-6 of Indole-3-carbinol in Cervical Cancer HeLa Cells
吲哚-3-甲醇新衍生物I3C-6对宫颈癌HeLa细胞生长的影响
The process is cheaper and simpler.
结论4羟基吲哚和4甲氧基吲哚的收率分别达574%288%,是值得研究推广的新工艺。
Indocin is the trade name of this nonsteroidal anti-inflammatory drug.
氯苯基甲氧基甲基吲哚乙酸是一种非固醇抗炎药物的商标名称。
Synthesis of 3,3-Dimethyl-2-(3-methylazulenevinyl)-3H-indole Derivative
3,3-二甲基-2-(3-甲基薁乙烯基)-3H-吲哚衍生物的合成
indolylalkylamine alkaloid
吲哚基烷基胺类生物碱
Eiectrosynthesis of Three Conducting Polymers with Carboxyl Group and Preparation of DNA Sensor Based on Poly(Indole-6-Carboxylic Acid) Films
三种含羧基导电聚合物的电合成及聚（6-羧基吲哚）DNA传感器的研制
Synthesis and in Vitro Antiviral Activities Against Influenza Viruses of Ethyl 5-Hydroxy-6-Bromo-1H-Indole-3-Carboxylate Derivatives;
5-羟基-6-溴吲哚-3-羧酸酯类化合物的合成及抗流感病毒活性研究
STUDY ON THE ENERGY TRANSFER PROCESS OF RE (Ⅲ)-1-ACETOACETYL-3-METHYLINDOLE COMPLEXE SYSTEM
1—乙酰乙酰基—3—甲基吲哚对稀土离子能量传递过程研究