Total yield of fosthiazate was as high as 36% andproduct purity was >80%.
先将2-噻唑烷酮与O,O'-二乙基硫代磷酰氯进行缩合反应生成O,O'-二乙基-2-氧代-1,3-噻唑烷-3-基硫逐磷酸酯,该硫逐磷酸酯再与二甲胺反应生成相应硫代磷酸酯铵盐,然后与溴代仲丁烷进行烷基化反应得到噻唑磷。
Overall yield of fosthiazate was as high as 44% and product purity determined by HPLC was >80%.
介绍了以三氯化磷、仲丁基二硫化物为原料反应得到O-乙基-S-仲丁基硫代磷酰氯,再与2-噻唑烷酮缩合得到噻唑磷的合成方法。
Fosthiazate is a novel non-fumigation-type organophosphate nematicide and soil insecticide with efficient, broad-spectrum.
噻唑磷是一种新颖、高效、广谱性的非熏蒸型有机磷杀线虫杀螨和土壤杀虫剂,是目前防治植物寄生线虫的理想药剂。
Study of Enantiomeric Pharmacokinetics of Dencichine Quality Criterion and Residue Monitoring of Fosthiazate;
三七素手性药物代谢动力学研究噻唑硫磷质量控制及残留监测
Solid-phase extraction (SPE) coupled with gas chromatography/mass spectrometry (GC/MS) was used to determine the fosthiazate residue in water samples.
建立了对环境水中噻唑硫磷农药残留进行检测的离线固相萃取 气相色谱/质谱联用(SPE GC/MS)的方法。
Determination of Fosthiazate by UV-VIS Spectrophotometry
紫外-可见分光光度法测定噻唑磷含量
The Synthesis Research and Process Design of 2-thiazolidinone, as Intermediate for Fosthiazate
新型杀线虫剂噻唑磷的关键中间体2-噻唑烷酮的合成研究与工艺设计
Study of Enantiomeric Pharmacokinetics of Dencichine Quality Criterion and Residue Monitoring of Fosthiazate;
三七素手性药物代谢动力学研究噻唑硫磷质量控制及残留监测
Determination of Guanoxan Sulfate and Chloroquine Phosphate Hydrochloride in Compound Dibazol and Hydrochlorothiazide Capsules by HPLC
HPLC法测定复方地巴唑氢氯噻嗪胶囊中硫酸胍生和磷酸氯喹的含量
STUDY ON SYNTHESIS AND TRIBOLOGICAL PROPERTIES OF A MULTIFUNCTIONAL NOVEL 2-MERCAPTOBENZOTHIAZOL DERIVATIVE
S-(2-巯基苯并噻唑)O,O′-二烷基二硫代磷酸酯的合成及性能研究
Synthesis of 2-Bromo-1,3,4-Thiadiazole
2-溴-1,3,4-噻二唑的合成
Synthesis of Aminothiazole and Thiazolidinone Derivatives in Ionic Liquid;
在离子液中合成氨基噻唑、噻唑琳酮类化合物
Synthesis of Spiro-Heterocycle Compounds of Oxazole, Thiazole and Quinoline Derivatives;
含噁唑、噻唑基螺杂环化合物的合成
Studies on the Synthesis of Thia/Oxadiazole and Triazole Compounds
噻（噁）二唑及三唑类化合物的合成研究
Synthesis of Thiazoline and Thiazine Thioethers & Study on Their Biological Activities;
噻唑啉和噻嗪类硫醚的合成及其生物活性研究
The solid-state phase reaction synthesis of copolymer with dithiophenyl-benzene and dithiophenyl-benzothiadiazole
二噻基苯和二噻基苯并噻二唑共聚物的固相合成
test method for total 2-mercaptobenzothiazole in benzothiazyl disulfide vulcanization accelerator
苯并噻唑基二硫化物中总2-硫醇苯并噻唑含量试验方法
test method for free 2-mercaptobenzothiazole in benzothiazyl disulfide
苯并噻唑基二硫化物中游离2-硫醇苯并噻唑含量测定方法
Design and Synthesis of Thiadiazole and Benzothiazole Compounds by Iodobenzene Diacetate;
应用二醋酸碘苯设计合成噻二唑类、苯并噻唑类杂环化合物
Synthesis and Bioactivity Study of Tertazole, Thiadiazole Heterocyclic Derivatives;
四唑、噻二唑杂环衍生物的合成及性质研究
Synthesis and Investigation on the Mesophase Property of New Oxadiazole and Thiadiazole Derivatives;
新型噁二唑、噻二唑衍生物的合成及液晶性研究
Syntheses of Thiazole Glycosyl Esters and Tetrazol Glycosides;
含有噻唑环的糖酯及四氮唑糖苷的合成
Synthesis of Glycosylamino and Benzothiazole Deteratives Bearing Aryltetrazole;
含芳基四唑糖氨基及苯并噻唑衍生物的合成